research paper

Application of the Linkam TS1400XY heating stage to melt inclusion studies

Melt inclusions offer a direct method to study magmatic processes and the evolution of magmatic systems, including the determination of volatile content in a magma body before an eruption. Various techniques, such as heating in one-atmosphere furnaces, high-pressure vessels, and microscope-mounted high-temperature stages, are used to homogenize MI for analysis. Discover how the Linkam TS1400XY heating stage revolutionises the study of melt inclusions with its exceptional ability to homogenize melt inclusions and swiftly quench the homogeneous melt into a glass, it opens up new possibilities for research and exploration.

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TS1400XY

Contactless probing of polycrystalline methane hydrate at pore scale suggests weaker tensile properties than thought using Linkam’s CAP500

Tensile properties of polycrystalline methane hydrate are analysed using Linkam’s CAP500 under microscopy.

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Wan, Ye, et al. "An Experimental Study of the Formation of Talc through CaMg (CO3) 2–SiO2–H2O Interaction at 100–200 C and Vapor-Saturation Pressures." Geofluids 2017 (2017).

Adaptive 3D cryogenic correlative light imaging of native biology using laser free confocal system

CMS196V4 shown above

Cryogenic light microscopy is an important part a correlative imaging workflow, allowing confirmation of localised molecules of interest prior to processing for downstream analysis such ultrastructural or compositional assessment. It is a key mapping step.

Here, the authors describe adaptation of a standard upright widefield microscope into a cryogenic 3D laser-free confocal system using Linkam’s CMS196, demonstrating the necessary sample preparation steps followed by confocal imaging of biological cells and tissues.

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Nizamudeen, Zubair Ahmed, et al. "Adaptive 3D cryogenic correlative light imaging of native biology using laser free confocal system. Wiley Analytical Science

Solar Cells Operating under Thermal Stress

Solar cells and photovoltaic devices are generally optimised for use at room temperature, but there are certain applications that find them in higher or lower temperature environments, such as in extraterrestrial exploration or in the hottest deserts. This review details examples of how temperature-controlled experiments play an important part in characterising and understanding the behaviour of next-gen photovoltaic devices, including some examples using Linkam’s electrical stages.

Read the full article here: https://www.cell.com/cell-reports-physical-science/fulltext/S2666-3864(20)30289-7

Rodolphe Vaillon, Stéphanie Parola, Chrysovalantou Lamnatou, Daniel Chemisana. “Solar Cells Operating under Thermal Stress” Cell Reports Physical Science 1, 100267 https://doi.org/10.1016/j.xcrp.2020.100267

Using Linkam’s TS1500 to investigate the influence of pretreatment parameters on the surface characteristics of amorphous metal for use in power industry

Researchers use Linkam’s TS1500 to investigate the properties of “metallic glasses”, or amorphous metals, as they undergo annealing at high temperature. These materials are potentially useful for the production of high efficiency energy devices.

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Heterogeneous oxidation of amorphous organic aerosol surrogates by O3, NO3, and OH at typical tropospheric temperatures

Researchers use Linkam’s BCS196 Cryobiology stage with optical microscopy to observe and measuree reactive uptake coefficients (γ ) of O3, NO3, and OH for several systems of oxidant and organic aerosol surrogate combinations.

Intrinsic mechanical behaviour of femoral cortical bone in young, osteoporotic and bisphosphonatetreated individuals in low - and high energy fracture conditions

Researchers used Linkam’s Modular Force Stage (MFS) to investigate treatments for osteoporosis in fractures of femoral bones.

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Zimmermann, E., Schaible, E., Gludovatz, B. et al. Intrinsic mechanical behavior of femoral cortical bone in young, osteoporotic and bisphosphonate-treated individuals in low- and high energy fracture conditions. Sci Rep 6, 21072 (2016). https://doi.org/10.1038/srep21072

Linkam’s TS1500 used to enable in situ study of sigma phase formation in Cr–Co–Ni ternary alloys at 800 °C at the long duration experiment facility at Diamond Light Source

Read how a unique setup using Linkam’s TS1500 allows researchers to perform beamline XRD analysis at high temperature at Diamond Light Source. Here, they use the new long-duration experimental beamline I11 to study phase formation kinetics of metal alloys, demonstrating a new technique for metallurgical studies.

Flow-induced crystallisation of polymers from aqueous solution using Linkam’s CSS450

Researchers used Linkam’s CSS450 to replicate the mechanical properties of natural silk by creating a synthetic polymer that solidifies when subject to flow. Using temperature-controlled shear in the aqueous phase they induce polymer crystallisation, providing an alternative low-energy polymer processing route.

Elastic response of (1−x)Ba(Ti0.8Zr0.2)O3 – x(Ba0.7Ca0.3)TiO3 (x=0.45–0.55) and the role of the intermediate orthorhombic phase in enhancing the piezoelectric coupling using Linkam’s HFS600E-PB4

Using Linkam’s HFS600E-PB4 Linkam probe stage at temperatures down to -70 °C (200K), this study looks at how temperature-dependent phase transitions affect the properties of piezoelectric materials, finding that ideal properties peaked around the low-temperature phase transitions.

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Optothermotronic effect as an ultrasensitive thermal sensing technology for solid-state electronics using Linkam’s HFS600E-PB4.

Researchers study the effect of thermal excitation on semiconducting sensor materials using a Linkam probe stage, the HFS600E-PB4. They explore the temperature sensing performance of these semiconductor nanofilms.